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1 article(s) from Zengerle, Michael

Highly efficient cyclosarin degradation mediated by a β-cyclodextrin derivative containing an oxime-derived substituent

Michael Zengerle,
Florian Brandhuber,
Christian Schneider,
Franz Worek,
Georg Reiter and
Stefan Kubik

Beilstein J. Org. Chem. 2011, 7, 1543–1554, doi:10.3762/bjoc.7.182

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Figure 1: Schematic representation of the general structural design of the investigated cyclodextrin derivati...

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Scheme 1: Structure of cyclosarin (GF).

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Scheme 2: Cyclodextrin derivatives tested as potential GF scavengers.

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Scheme 3: General strategies used for the preparation of the investigated cyclodextrin derivatives.

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Scheme 4: Reaction conditions used for the preparation of cyclodextrin derivatives 1a–e from tosylate 3.

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Scheme 5: Synthesis of 3-(aminomethyl)benzaldehyde oxime (5). Reagents and conditions: i. NaBH₄, EtOH, 1 h, 2...

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Scheme 6: Synthesis of 3-((hydroxyimino)methyl)-1-(prop-2-ynyl)pyridinium bromide (6). Reagents and condition...

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Scheme 7: Syntheses of 6-ethynyl-formylpyridine oximes (7a–c). Reagents and conditions: i. CuI, (PPh₃)₂PdCl₂,...

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Scheme 8: Reaction conditions used for the preparation of cyclodextrin derivatives 2a–d from azide 4.

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Figure 2: Diagram summarizing the observed Δk₁ values for cyclodextrins 1a–e and 2a–d. For comparison, the re...

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Figure 3: Time-dependent decrease of GF concentration in the presence of 1b (top row), 1c (middle row), and 2a...

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Scheme 9: Schematic protocol for the qualitative assay.

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Scheme 10: Schematic protocol of the quantitative assay.

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Published 22 Nov 2011

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